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Formation of meta-Arylsulfanyl- and meta-(Alkylsulfanyl)phenols from Cyclohexane-1,3-diones
Download2018-01-01
Thanh, Nhan Do Van, Patra, Subrata, Clive, Derrick L. J.
Reaction of cyclohexane-1,3-diones with TsCl/Et3N and treatment of the resulting 3-(tosyloxy)cyclohex-2-en-1-ones with aryl- or alkyl thiols and K2CO3 in MeCN gives 3-(arylsulfanyl)cyclohex-2-en-1-ones or (alkylsulfanyl)cyclohex-2-en-1-ones, respectively. These compounds are easily brominated at...
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