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Pitch Production Using Solvent Extraction of Coal: Suitability as Carbon Anode Precursor

  • Author / Creator
    Mohammad Ali Pour, Mehdi
  • Albertan coal has been used to produce extracts as precursor for production of anode coke. Coal extractability was studied using digestion with Tetralin in a 500 ml reactor. Different operating conditions were tried and optimum conditions were chosen for runs with coal-derived solvents. Extracts from runs with coal-derived solvents and their hydrotreated versions were distilled and heat treated to produce pitches as coke precursors. Coking experiments were performed using a molten salt bath furnace. Coal, solvents, pitches and cokes were characterized to study the effects of process chemistry on coke anisotropy. Coke anisotropy was studied using image analysis of polarized light optical micrographs and x-ray diffraction. Aromaticity of the pitch was found to be the key parameter controlling coke anisotropy. Solvent was found to be the most important factor contributing to pitch aromaticity. Heat treated products of high aromaticity yield the highest coke conversion and anisotropy.

  • Subjects / Keywords
  • Graduation date
    2009-11
  • Type of Item
    Thesis
  • Degree
    Master of Science
  • DOI
    https://doi.org/10.7939/R39694
  • License
    This thesis is made available by the University of Alberta Libraries with permission of the copyright owner solely for non-commercial purposes. This thesis, or any portion thereof, may not otherwise be copied or reproduced without the written consent of the copyright owner, except to the extent permitted by Canadian copyright law.
  • Language
    English
  • Institution
    University of Alberta
  • Degree level
    Master's
  • Department
    • Department of Chemical and Materials Engineering
  • Supervisor / co-supervisor and their department(s)
    • Rajender Gupta, Chemical and Materials Engineering, University of Alberta
  • Examining committee members and their departments
    • Amit Kumar, Mechanical Engineering, University of Alberta
    • Arno de Klerk, Chemical and Materials Engineering, University of Alberta