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Lead‐207 NMR spectroscopy at 1.4 T: Application of benchtop instrumentation to a challenging I = ½ nucleus
Download2020-01-01
Bernard, G.M., Michaelis, V.K.
The practicality of obtaining liquid‐ and solid‐state 207Pb nuclear magnetic resonance (NMR) spectra with a low permanent‐field magnet is investigated. Obtaining 207Pb NMR spectra of salts in solution is shown to be viable for samples as dilute as 0.05 M. The concentration dependence of the 207Pb...
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2017-01-01
Bernard, G.M., Goyal, A., Miskolzie, M., McKay, R., Wu, Q., Wasylishen, R.E., Michaelis, V.K.
A new solid-state nuclear magnetic resonance (NMR) thermometry sample is proposed. The 207Pb NMR chemical shift of a lead halide perovskite, methylammonium lead chloride (MAPbCl3) is very sensitive to temperature, 0.905 ± 0.010 ppm K−1. The response to temperature is linear over a wide...