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- 24Chemistry
- 23Organic compounds. Synthesis.
- 22Metabolomics
- 21Capillary electrophoresis.
- 21Catalysis
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Improved Gram-Scale Procedure for MIBA-Catalyzed Direct Amidation and Its Application to the Preparation of alpha and beta Peptides
DownloadFall 2015
Direct condensation between a carboxylic acid and amine must overcome the initial formation of a thermodynamically stable and unreactive carboxylate-ammonium salt, providing the amide product only at very high temperatures (over 160 oC) that are incompatible with many functionalized molecules....
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Improving the spectral stability of poly(9,9-dioctylfluorene) (PFO) through the use of aromatic ethers
DownloadSpring 2011
Aromatic ethers (AEs) have been combined with poly(9,9-dioctylfluorene) (PFO) to improve spectral stability in PFO systems. Compared to neat PFO, PFO/AE blends were found to have decreased ‘g-bands’ following heating in air. Some were further found to induce and maintain β-phase emission. The...
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In vitro compartmentalization and deep sequencing enable discovery of functional cell-binding ligands by phage display
DownloadFall 2015
Phage display is a technique that accelerated the discovery of peptide and protein-based ligands to numerous targets in academia and industry. Many FDA-approved antibodies and peptides on the market have originated from phage display experiments. However, one of the main drawbacks to this...
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In-Situ Spectroscopic Characterization of Operating Polythiophene Nonvolatile Memory Devices
DownloadSpring 2014
Au/P3HT/PEO-EV(ClO4)2/C/Au nonvolatile memory devices were developed based on resistive switch of conducting polymers in the solid state. The P3HT layer was switched using a “write/erase” bias, while internal composition of the device was monitored using in-situ UV-Vis absorbance spectrometer...
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Fall 2011
The first chapter of this thesis describes the development of an asymmetric route to the core structure of the indolizidine alkaloids and its application to the total synthesis of (+)-ipalbidine, a member of this compound class. The initial approach was designed to use the intramolecular...
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Spring 2020
Sialic acids are an incredibly diverse family of carbohydrates that serve many roles in biological systems. Their presentation is influenced not only by structural modification of the sialic acid, but also by attachment through glycosidic linkages and their presence on different glycoconjugates....