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- 24Chemistry
- 23Organic compounds. Synthesis.
- 22Metabolomics
- 21Capillary electrophoresis.
- 21Catalysis
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Multifunctional Carbazole-Based Materials as Electrochemical Water Splitting and Photoredox Catalysis
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The combustion of fossil fuels releases carbon dioxide and other harmful greenhouse gases into our living atmosphere, which traps heating and causes global warming. Renewable energy, however, can help solve the problem above by producing far fewer greenhouse gases. Renewable energy is a general...
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Spring 2023
In this thesis, rare-earth-containing chalcogenides and oxychalcogenides were sought with the aim to identify new crystal structures and to evaluate their potential as optical and thermoelectric materials. They were synthesized in the form of pure microcrystalline powders and single crystals...
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Investigating the Early Phases of Aerosol Particle Nucleation: A Broadband Rotational Spectroscopic and Computational Study
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Atmospheric aerosols consist of solid or liquid particles suspended in air with sizes ranging from a few nanometers to several micrometers. Aerosols have the ability to both scatter and absorb incoming solar radiation, directly influencing Earth’s energy budget and resulting in either cooling or...
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Spring 2023
Catalysis is essential to the modern chemical industry. Catalytic strategies can enable new synthetic methods with improved atom economy and reduced chemical waste under mild conditions, representing an indispensable approach to the development of green chemical processes with improved...
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Environmental Monitoring: Utilizing Efficient Extraction, Separation, and Detection Methods for Application in Routine and Specialized Analyses
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Environmental analysis is a field that has made significant progress in academic research over the last number of years. Whether it be sampling techniques, sample introduction, separations, or analytical instrumentation, there seems to be no shortage of ideas and innovation to improve the way...
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Fall 2023
Three new Re(I) photocatalysts were prepared by synthesizing imidazole and imidazolium dyes based on carbazolyl dicyanobenzene derivatives and physically linking them to a Re metal centre for the photochemical reduction of CO2. The imidazolium dyes were of interest because they are precursors to...
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Development of New Late-Stage Labeling Methods with Labeled Carbon for Stabilized Carboxylic Acids and α-Amino Acids
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Isotope labeling of small molecules is a crucial tool for drug discovery and understanding biochemical processes. Expanding the toolbox of a radiochemist with methods that allow late-stage labeling is therefore important. Of the methods that have been developed, the use of isotopically labeled...
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Fall 2023
This thesis describes the synthesis of Li-containing intermetallics and chalcogenides using high-temperature solid-state reactions and induction heating, with the aim of studying their structures, electronic properties, and optical properties to gain insights into their potential applications in...
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Insights on local chemical structure of chalcogenide photovoltaic materials using solid state NMR spectroscopy
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Quaternary chalcogenides with the formula I2-II-IV-VI4 have emerged as promising candidates for photovoltaic materials, but many details about their structures remain poorly understood. This thesis describes the synthesis, structure determination, and optical properties of the sulfides Cu2MTtS4...