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Mechanochemical Synthesis of Methylammonium Lead Mixed–Halide Perovskites: Unraveling the Solid-Solution Behavior Using Solid-State NMR
Download2018-01-01
Karmakar, A., Askar, A.M., Bernard, G.M., Terskikh, V.V., Ha, M., Patel, S., Shankar, K., Michaelis, V.K.
Mixed-halide lead perovskite (MHP) materials are rapidly advancing as next-generation high-efficiency perovskite solar cells due to enhanced stability and bandgap tunability. In this work, we demonstrate the ability to readily and stoichiometrically tune the halide composition in...
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Multinuclear Magnetic Resonance Tracking of Hydro, Thermal and Hydrothermal Decomposition of CH3NH3PbI3
Download2017-01-01
Askar, A.,, Bernard, G.M, Wiltshire,, B., Shankar, K., Michaelis, V.K.
An NMR investigation of methylammonium lead iodide, the leading member of the hybrid organic-inorganic perovskite class of materials, and of its putative decomposition products as a result of exposure to heat and humidity, has been undertaken. We show that the 207Pb NMR spectra of the compound of...